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molybdenum carbide synthesis

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Facile synthesis of high surface area molybdenum …

Molybdenum carbide has immense potential as an active catalyst for reaction systems such as synthesis of important chemicals like ammonia. However, the carbide is not used as a commercial catalyst or support as the current synthesis processes produce low surface area material or have contaminants such as excess carbon and surface and chemisorbed oxygen.

Facile Synthesis and Thermal Stability of …

Nanocrystalline molybdenum carbide (Mo2C) was prepared via one simple route by the reaction of metallic magnesium powders with molybdenum trioxide and potassium acetate in an autoclave at the condition of 600℃ and 4 h. X-ray powder diffraction (XRD) pattern indicated that the product was hexagonal α-Mo2C, and the cell constant was a = 3.0091 Å, c = 4.7368 Å.

Synthesis, characterization, and activity of …

Abstract: Early transition metal nitrides and carbides, including molybdenum carbide, have been found to have catalytic properties that are competitive with those of more conventional catalysts for a variety of reactions, including alkane conversion and the hydrotreatment of organonitrogen and organosulfur compounds. The goal of the research described in this dissertation was to understand the ...

Synthesis of Nanostructured Molybdenum Carbide as …

The effect of the morphology and size of unsupported molybdenum carbide (β-Mo2C) was investigated in the selective hydrogenation of levulinic acid to γ-valerolactone (GVL) in aqueous phase. Nanostructured β-Mo2C was synthetized by two different approaches: (i) using multiwalled carbon nanotubes (CNT) as both hard template and source of carbon and; (ii) using 1D nanostructured α-MoO3 as ...

Synthesis of molybdenum carbide catalyst by DC arc …

According to the X-ray diffraction data, two molybdenum carbide phases are identified in the powder synthesis product: Mo1.2C0.8 and Mo2C, as well as graphite and metallic molybdenum.

2D molybdenum and vanadium nitrides synthesized …

Synthesis of two-dimensional molybdenum carbide, Mo 2 C, from the gallium based atomic laminate Mo 2 Ga 2 C journal, November 2015 Meshkian, Rahele; Näslund, Lars …

Molybdenum carbide synthesis using plasmas for fuel …

Molybdenum carbide synthesis using plasmas for fuel cells ...

Synthesis and Characterization of Molybdenum …

Laser radiation (XeCl laser, 308-nanometer wavelength) focused into a cell containing Mo(CO)6 vapor produced ultrafine particles in the extended waist of the laser beam. Negative ion mass spectrometry revealed molybdenum carbide cluster ions with a stoichiometry Mo n C4 n ( n = 1 to 4). The Mo n C4 n – ( n = 2 to 4) ions are completely unreactive with NH3, H2O, and O2, suggesting structures ...

Synthesis and Characterization of Molybdenum …

Laser radiation (XeCl laser, 308-nanometer wavelength) focused into a cell containing Mo(CO)6 vapor produced ultrafine particles in the extended waist of the laser beam. Negative ion mass spectrometry revealed molybdenum carbide cluster ions with a stoichiometry Mo n C4 n ( n = 1 to 4). The Mo n C4 n – ( n = 2 to 4) ions are completely unreactive with NH3, H2O, and O2, suggesting structures ...

Synthesis and characterization of massive …

Procedures for the synthesis of massive molybdenum carbide by the mechanical activation of a mixture of MoO3, commercial carbon, and Zn in air and the synthesis of the supported carbide-containing catalyst Mo2C/C by the mechanical activation of commercial carbon impregnated with a 16% aqueous solution of ammonium paramolybdate in an inert atmosphere were developed for the first time. With the ...

A facile one-step synthesis of molybdenum carbide …

2020-7-27 · A molybdenum carbide-carbon composite (β-Mo 2 C/C) is prepared by carbonization of an anionic resin with molybdate. The β-Mo 2 C/C is characterized by X-ray diffraction, N 2 physisorption, scanning electron microscopy, and transmission electron microscopy. Characterization indicates that the sample shows a hierarchically microporous, mesoporous, and macroporous structure, and has a large ...

ON THE SYNTHESIS OF MOLYBDENUM CARBIDE …

This paper aims to evaluate the synthesis and characterization of molybdenum carbide with low Co addition (Co/Mo=2.5 and 5 mol%) at two temperature levels (700 and 750 °C) by using a carburizing/ reducing atmosphere with low CH 4 content (5%) in order to avoid free carbon formation.

ON THE SYNTHESIS OF MOLYBDENUM CARBIDE …

This paper aims to evaluate the synthesis and characterization of molybdenum carbide with low Co addition (Co/Mo=2.5 and 5 mol%) at two temperature levels (700 and 750 °C) by using a carburizing/ reducing atmosphere with low CH 4 content (5%) in order to avoid free carbon formation.

Pechini synthesis and characterization of molybdenum ...

Pechini synthesis and characterization of molybdenum carbide and nickel molybdenum carbide Stux, Arnold M.; Laberty-Robert, Christel; Swider-Lyons, Karen E. Abstract. Carbides, such as η-Ni 6 Mo 6 C, are considered as low-cost substitutes for noble metal catalysts for present applications in hydrodesulfurization and for a possible future ...

Pechini synthesis and characterization of molybdenum ...

Pechini synthesis and characterization of molybdenum carbide and nickel molybdenum carbide Stux, Arnold M.; Laberty-Robert, Christel; Swider-Lyons, Karen E. Abstract. Carbides, such as η-Ni 6 Mo 6 C, are considered as low-cost substitutes for noble metal catalysts for present applications in hydrodesulfurization and for a possible future ...

Self‐assembly‐ and Preshaping‐assisted Synthesis of ...

Abstract Herein, we report a self‐assembly and preshaping strategy for the controllable synthesis of highly dispersed Mo2C nanoparticles supported on porous graphitic carbon lamellas. This simple b...

Frontiers | Hierarchical Porous Molybdenum Carbide …

The electrocatalytic hydrogen evolution reaction (HER) for the preparation of hydrogen fuel is a very promising technology to solve the shortage of hydrogen storage. However, in practical applications, HER catalysts with excellent performance and moderate price are very rare. Molybdenum carbide (MoxC) has attracted extensive attention due to its electronic structure and natural abundance.